A Libertarian-Conservative Case Against Identity Cards by Sean Gabb

By Sean Gabb

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Co(Ars)2(CO)NO] (M-20), IR spectrum - NO valence vibration (135). (Ars)CO~S-~CF3J 1S- CCF3 ,brown, paramagnetic crystals, m. 5-188°, prepd. 2 from [COS4C4(CF4)4J2 + Ars in dry C5H~2' Polarographic data, electronic and ESR spectra; a square-pyramidal structure for the 5-coordinate Co was suggested (110). [Co(Ars) [ON=C(Me)C(Me)=NOBPh2]2} , red-brown crystals, m. 192-195°, prepd. from {Co(Ars)[ON=C(Me)C(Me)=NOH]2Cl} in THF by treating the soln. with K (1:2) under reflux, followed by Ph2BCl and completing the rxn.

177°, electronic spectrum - the effect of the Me groups and of so 1vents (423). : {Mn[ArS(CeH2Me3)3]2(CO)3I}, prepd. from Mn(CO)sI by heating with the arsine. Sol. in hydrocarbons, useful as an antiknock additive (1612). Trinaphthylarsine, AsC30H21, (ClOH-r bAs, (M-32) Uses: A stabilizer for photochromic systems such as the mixts. of 2,3-diphenylindenone 2,3-epoxide in poly(methyl methacrylate) against mol. degradation (1544). Complexes with M[AlI4] (M = alkali metal) and Ti, V, Zr, Cr, or Mo halides catalyze the polymerization of a-olefins (385).

With Ph3P - displacement of one CO group (1652). cis-[Re(Ars)(PPh3)(CO)3Cl], prepd. from cis-[Re(Ars)(CO)4Cl] + Ph3P in MePh at 70·. The rate of rxn. was detn. by means of the changes of the IR spectrum of the rxn. mixt. (1652). , formed from [Et4N]2[ReHs] + Ars in i-PrOH under reflux; the liq. phase cont. [Et4N][ReHa(Ars)] (619). Et4N[ReHa(Ars)], white cryst. , a 1:1 electrolyte in MeCN, prepd. as described above along with [ReHs(ArS)3] and sepd. from the liq. phase by evapn. to dryness. IR and NMR.

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